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Zinc-mediated reactions on salicylaldehyde for Botrytis cinerea control, Chinese Chemical Letters, 2019. ,
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, 75% yield. 1 H NMR (400 MHz, 2019.
,
3 Hz); 6.92 (2H, d, J = 8.8 Hz); 2.68 (2H, t ,
CDCl 3 ): ? 7.86 (2H, d, J = 8.6 Hz); 7.8 (2H, d, J = 8.1 Hz), vol.7, issue.400 ,
, 7 mmol) filtration under vacuum, the solvent was evaporated. The residue was purified by silica gel chromatography, Cyclohexane/EtOAc, vol.19
, ×2); 69.6; 61.3. 2b (orange solid, 3.58 g, 67% yield) mp = 126°C, 1 H NMR (400 MHz
, FTIR: 3334 cm ?1 (w), 2931 cm ?1 (w), 1597 cm ?1 (s), 1500 cm ?1 (s), 1252 cm ?1 (s), 1079 cm ?1 (s), 1045 cm ?1 (s), pp.841-842
, 2c [37] (orange solid, 1.98 g, 34% yield) 1 H NMR (400 MHz, HRMS (ESI+) m/z calculated for
,
, Synthesis of a 3a-3d To a solution of 2a-2d (4 mmol) dichloromethane (25 mL), tri
, Compounds 3a-3d was dissolved in a H 2 O/acetone mixture (2:1)
,
,
,
,
1 Hz), vol.7, p.36 ,
,
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, , vol.7, p.33
, AZOTAI 4d orange solid, 495 mg, 25% yield. mp = 196°C 1 H NMR (400 MHz, MeOD) 7.92 (2H, d, J = 8.7 Hz), vol.7
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Unlocking structure-self-assembly relationships in cationic azobenzene photosurfactants, Langmuir, vol.34, pp.10123-10134, 2018. ,
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Hydrophobic study of increasing alkyl chain length of platinum surfactant complexes: synthesis, characterization, micellization, thermodynamics, thermogravimetrics and surface morphology, RSC Adv, vol.6, issue.93, pp.90607-90623, 2016. ,
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